The AD rat models were established by injecting amyloid-beta peptide ( A β _ 25-35 ) into right amygdala . The sham-operation rats were injected with trifluoroacetic acid in the same location .
右侧杏仁核注射β淀粉样肽(Aβ2535)制备AD大鼠模型,假手术组同样部位注射 三 氟 乙酸;
Diacetone acrylamide was synthesized with acrylonitrile and acetone as raw material and with trifluoroacetic acid and concentrated sulfuric mixed acid as catalyst .
以丙烯腈和丙酮为原料, 探索以 三 氟 乙酸和浓硫酸组成的混酸作催化剂合成双丙酮丙烯酰胺工艺。
Trifluoroacetic acid can cause redshift of UV-Vis absorption spectra and great enhancement of the fluorescent intensity at 433 nm owing to the effect of protonation .
用 三 氟 乙酸质子化,可引起紫外-可见吸收光谱的红移以及433nm处荧光强度的显著增强。
Three . Synthesis and application of trifluoroacetic acid
三 氟 乙酸的制备及应用
Methods 3-Fluoro-4-methoxybenzaldehyde was prepared through the reaction of 2-fluoroanisole with hexamethylenetetramine in the presence of trifluoroacetic acid and then extracted with anhydrous ether from the mixture after basification with potassium carbonate .
方法以 三 氟 乙酸为溶剂,邻氟苯甲醚与六次甲基四胺发生回流反应,通过无水碳酸钾调节酸碱度、无水乙醚萃取等操作制备3氟4甲氧基苯甲醛。
For the oxidation reaction under the conditions of 24h and room temperature the volume proportion of trifluoroacetic acid and H_2O_2 ∶ 10 .
氧化反应:室温条件下氧化24h, 三 氟 乙酸与双氧水的体积比为1∶10。
Trifluoroacetic acid ( TFA ) was used as the retaining acid and ammonia liquor as the eluent base . The solvent system was n-hexane-acetic ester-methanol-water ( ratio by volume was 9 ∶ 1 ∶ 5 ∶ 5 ) .
采用 三 氟 乙酸做为保留酸,氨水作为洗脱碱,溶剂系统为正己烷/乙酸乙酯/甲醇/水(体积比为9∶1∶5∶5)。
In this paper some mixed ligand complexes of rare earth with 1 and trifluoroacetic acid were synthesized in aquo-organic solvent . The composition of complexes is Ln ( CF3COO ) 3 ·( Phen ) 3 · nH2O .
本文在含水溶剂中合成得到稀土 三 氟 醋酸盐 与 三份邻菲罗啉配位的配合物,确定其组成为Ln(CF3COO)3·(Phen)3·nH 2O。
When SiO2-g - ( PCL-b-PtBA ) nanohybrids were subjected to hydrolysis with trifluoroacetic acid pH-sensitive SiO2-g - ( PCL-b-PAA ) hybrid materials were obtained whose surface charge numbers and sizes of aggregates at different pH values were quite different .
将SiO2-g-(PCL-b-PtBA)纳米杂化材料进行水解,得到了具有pH敏感性的 SiO2-g-(PCL-b-PAA)杂化材料,其表面电荷和聚集体尺寸大小随pH值的改变而显著不同。
The chromatographic conditions are as follows : ODS-AM-303 column ( YMC 4.6mm × 250mm 5 μ m ) with the temperature of 40 ℃ acetonitrile-water ( 40:60 ) containing 0.1 % trifluoroacetic acid as mobile phase with the flow rate of 1mL / min.
色谱条件为:ODS-AM-303色谱柱(YMC,4.6mm×250mm,5μm),柱温40℃,含0.1% 三 氟 乙酸的乙腈-水(40∶60)为流动相,流速1mL/min。
03012801 as analytic column methanol-0.1 % trifluoroacetic Acid ( 60 ∶ 40 ) as mobile phase the flow rate being 1.0 ml · min ~ - 1 the detection wavelength at 273 nm .
03012801为色谱柱,甲醇∶0.1% 三 氟 乙酸水溶液(60∶40)为流动相;流速:1.0ml·min-1;
Study on Growth and Properties of Trifluoroacetic Acid Doped TGS Crystals
掺 三 氟 乙酸TGS晶体生长及其性能研究
METHOD HPLC method was used to carry out the determination with C 18 Column methanol-0.1 % trifluoroacetic acid water solution as the mobile phase ( 75 ∶ 72 ) and a wavelength of 293 nm .
方法采用HPLC法,C18柱,流动相为甲醇0.1% 三 氟 乙酸水溶液(75∶25),检测波长为293nm。
The mobile phase was ( A ) aqueous trifluoroacetic acid solution ( 0.2 % ) solution and ( B ) acetonitrile trifluoroacetic acid solution ( 0.1 % ) . The gradient elution was modified as follows : initial 10 % B ;
流动相:A相为0.2%的 三 氟 乙酸水溶液,B相为含0.1%的三氟乙酸的乙腈溶液,线性梯度程序为:开始10%B;
The mobile phase was consisted of 1 % trifluoroacetic acid solution as mobile phase A and acetonitrile - methanol ( 75:25 ) as mobile phase B with UV detection at 275 nm .
流动相A为1%的 三 氟 乙酸溶液,B为乙腈-甲醇(75:25);
Preparation and Tribological Properties of TiO_2 Nanoparticles Modified by Trifluoroacetic Acid
三 氟 乙酸修饰TiO2纳米微粒的制备及磨擦学性能
An unambiguous assignment of the main 1H NMR resonance of nylon 6 in trifluoroacetic acid ( TFA ) solution was carried out by using a combination of 1D and 2D NMR heteronuclear technique ( HMQC ) .
采用1D和2DNMR技术,归属了 三 氟 乙酸(TFA)溶液中尼龙6链上的主要1HNMR共振信号。
Nuclear Magnetic Resonance Relaxation of Cohesional Entanglement of Nylon 6 Chains in Trifluoroacetic Acid Solution
三 氟 乙酸溶液中尼龙6链凝聚缠结的NMR弛豫研究
The capacitors prepared with PPy-DEHS ( PPy powder doped with di ( 2-ethylhexyl ) sulfosuccinate sodium salt ) electrolyte in trifluoroacetic acid show high capacitance and low tan δ .
应用PPy-DEHS(2-(2-乙基己基)硫代丁二酸钠盐掺杂聚吡咯,溶剂为 三 氟 乙酸)电解质装配的固体钽电解电容器具有较高的电容量和较低的损耗。
This study was focused on the determination of trace trifluoroacetic acid ( TFA ) with derivation-gas chromatography .
本文研究了水中微量 三 氟 乙酸(TFA)的衍生化-气相色谱检测方法。
Finally in the methylation reaction of S-adenosyl methionine anisole was used in the extraction process of trifluoroacetic acid then distilled to recover the trifluoroacetic acid .
在甲基化生成S-腺苷蛋氨酸的反应完成后,用苯甲醚来萃取反应过程中使用的 三 氟 乙酸,萃取液蒸馏后,得到回收的三氟乙酸。
Trifluoroacetic acid accounted for half of the cost of in the synthesis process of LLM-105 so the recycle is with high economic value .
我们对LLM-105生成过程中的 三 氟 乙酸进行了回收,但效果不理想, 三 氟 乙酸占了整个LLM-105生成的一半成本,对其回收有很高的经济价值。
To trifluoroacetic acid as a catalyst in solvent-free under the condition of the THC for three cyclopentadiene isomerization .
以 三 氟 甲 磺酸为催化剂,在无溶剂的条件下对四氢三环戊二烯进行异构化反应。
Investigated the effects of methoxylation reaction the different nitration system the different amination system and the volume proportion of trifluoroacetic acid and hydrogen peroxide on the total yield of LLM-105 .
对LLM-105的工艺改进方面研究了甲氧基化、不同硝化体系、氨化条件、 三 氟 乙酸与双氧水的体积比等因素对LLM-105总产率的影响,并优化了合成条件,确定了最佳工艺条件。
This method saves the use of drugs trifluoroacetic acid and greatly reducing the cost of MC detection because it can shorten the running time . So the method significantly reduce the cost of MC detection when it is compared with the water method of MC determination of national standards .
此方法较水中MC测定的国家标准方法,不仅省去 三 氟 乙酸的使用,运行时间还得以缩短,大大降低MC检测的成本。
Trifluoroacetic acid pyridine salt ;
三 氟 乙酸吡啶鎓;
Trifluoroacetic acid ( TFA ) is degradation product of some CFCs alternatives such as HFC-134a which has some inhibitory effects on plants and soil microbial communities .
三 氟 乙酸是HFC-134a等氯氟烃替代品的降解产物,对植物和土壤微生物群落的生长有一定抑制作用。
And then used high performance liquid chromatography ( RP-HPLC ) to analyze trifluoroacetic acid residues and related substances and after aseptic testing we inspected the quality of products .
然后使用反相高效液相色谱(RP-HPLC)对 免疫 九 肽 的 三 氟 乙酸残留和有关物质进行分析,之后进行无菌检测,考察了产品质量。
三氟乙酸